Synthesis of Reduced Graphene Oxide (RGO) by Using Hydrothermal Method

Authors

  • Monika S. Khole  Department of Physics, Kalikadevi Arts, Commerce & Science College, Shirur (K.), Dist-Beed-413249, Maharashtra, India
  • Sanjay K. Tupe  Department of Physics, Kalikadevi Arts, Commerce & Science College, Shirur (K.), Dist-Beed-413249, Maharashtra, India

Keywords:

Graphene oxide (GO), Reduced graphene oxide (RGO), Hydrothermal method, Improved Hummer Method, Raman Spectroscopy.

Abstract

Reduced graphene oxide, RGO (also called chemically modified graphene, CMG) was synthesized by a hydrothermal method, with graphite oxide (GO), prepared by using improved hummer method at different temperatures, served as the raw material. Structural and morphological studies indicate the degree of reduction is dependent on the temperature, which is also verified by Raman analysis. The variation in interlayer distance and the intensity ratio of the D to G Raman modes (ID/IG)indicates higher reaction temperature can accelerate more reduction of GO and also (I2D/IG) ratio indicate the reduction in number of graphene layers. The reduction material is characterization by Raman spectroscopy.

References

  1. Paulchamy B, Arthi G &Lingesh BD, ISSN: 2157-7439 JNMNT.
  2. Sasha Stankovich, Dmitriy A. Dikin, Richard D. Piner, Kevin A. Kohlhaas, Alfred Kleinhammes, Yuanyuan Jia, Yue Wu, SonBinh T. Nguyen, Rodney S. Ruoff; Carbon 45 (2007) 1558-1565.
  3. M.D Stoller, S. Park, Y. Zhu, J. An, R.S. Ruof, Nano Lett. 8 (2008) 3498-3502.
  4. B. Seger, P.V. Kamat, J. Phys. Chem. C 113 (2009) 7990-7995.
  5. Q. Yan, B. Hung, J. Yu, F, Zheng,J. Zang, J. Wu, B.L. Gu, F. Liu, W. Duan, Nano Lett. 7 (2007) 1469-1473.
  6. Songfeng Pei, Hui-Ming Cheng, Carbon 50 (2012) 3210-3228.
  7. Xiufeng Mei, Xiuqing Meng, Fengmin Wu, X. Mei et al. / Physica E 68 (2015) 81-86.
  8. Dachao Luo, Guoxin Zhang, JunfengLiu,XiaomingSun,dx.doi.org/10.1021/jp110001y|J.Phys. Chem. C 2011, 115, 11327-11335.
  9. Daniela C. Marcano, Dmitry V. Kosynkin, Jacob M. Berlin, Alexander Sinitskii, Zhengzong Sun, Alexander Slesarev, Lawrence B. Alemany, Wei Lu, James M. Tour, VOL.4. NO. 8-4806-4814. 2010.
  10. Handbook of Hydrothermal Technology/ by K. Byrappa and Masahiro Yoshimura.https://doi.org/10.1016/C2009-0-20354-0.
  11. Jinpyo Hong, Min Kyu Park, Eun Jung Lee, DaeEung Lee, Dong Seok Hwang &Sunmin Ryu, 3:2700| DOI: 10.1038/srep02700.
  12. Surajit Some, Youngmin Kim, Yeoheung Yoon, HeeJounYoo, Saemi Lee, Younghun Park &Hyoyoung Lee, 3: 1929| DOI: 10.1038/srep019291
  13. Basic Principle, Working and Instrumentation of Experimental Techniques, [Nikita H.Patel/ Ph.D Thesis /Sardar Patel University/ July-2015].

International Journal of Scientific Research in Science, Engineering and Technology

Downloads

Published

2021-07-25

Issue

Volume 9, Issue 5, July-August-2021

Section

Research Articles

License

Copyright (c) IJSRSET

Creative Commons License

This work is licensed under a Creative Commons Attribution 4.0 International License.

How to Cite

[1]
Monika S. Khole, Sanjay K. Tupe "Synthesis of Reduced Graphene Oxide (RGO) by Using Hydrothermal Method " International Journal of Scientific Research in Science, Engineering and Technology (IJSRSET), Print ISSN : 2395-1990, Online ISSN : 2394-4099, Volume 9, Issue 5, pp.85-88, July-August-2021.