Extraction of Oil from Plants
DOI:
https://doi.org/10.32628/IJSRSET2411435Keywords:
Black seed oil, Soxhlet extraction, Cyclohexane, Seed grinding, controlling stapeAbstract
Black seed oil is a natural oil extracted from the seeds of Nigella sativa; a flowering plant was used as a case study of the recovery of oil from plants. This project is interested in the recovery of black seed oil using the Soxhlet apparatus with ethanol and cyclohexane as solvents. The extracted oil was weighed after one, three, and six extraction cycles for both solvents. Results indicated that the weight of the oil extracted increased significantly in the third and sixth cycles compared to the first. Subsequently, the black seeds were ground, and the extraction process was repeated using only ethanol as the solvent. This modification demonstrated an enhanced extraction efficiency. The findings suggest that the grinding of black seeds prior to Soxhlet extraction with ethanol as a solvent could be a more effective method for oil yield. The study provides valuable insights into the optimization of black seed oil extraction, which could be beneficial for industrial applications. The controlling step also studied and it was found that the mass transfer is the controlling step due to changes in the recovery when using different particle size and solvent.
Downloads
References
R. Ferizi, M. F. Ramadan, e Q. Maxhuni, “Black Seeds (Nigella sativa) Medical Application and Pharmaceutical Perspectives”, J Pharm Bioallied Sci, vol. 15, no 2, p. 63–67, abr. 2023, doi: 10.4103/jpbs.jpbs_364_22. DOI: https://doi.org/10.4103/jpbs.jpbs_364_22
H. Hosseinzadeh, A. Tavakkoli, V. Mahdian, e B. M. Razavi, “Review on Clinical Trials of Black Seed (Nigella sativa) and Its Active Constituent, Thymoquinone”, J Pharmacopuncture, vol. 20, no 3, p. 179–193, set. 2017, doi: 10.3831/KPI.2017.20.021. DOI: https://doi.org/10.3831/KPI.2017.20.021
P. B. Tulayakul Alongkot; Kasemsuwan Suwicha; Wiriyarampa Srisamai; Pankumnoed Juree; Tippayaluck Suwanna; Hananantachai Hathairad; Mingkhwan Ratchaneekorn; Netvichian Ramnaree; Khaodhiar Sutha, “Comparative study of heavy metal and pathogenic bacterial contamination in sludge and manure in biogas and non-biogas swine farms”, J Environ Sci (China), vol. 23, no 6, p. 991–997, 2011, doi: 10.1016/s1001-0742(10)60484-6. DOI: https://doi.org/10.1016/S1001-0742(10)60484-6
E. M. Yimer, K. B. Tuem, A. Karim, N. Ur-Rehman, e F. Anwar, “Nigella sativa L. (Black Cumin): A Promising Natural Remedy for Wide Range of Illnesses”, Evidence-Based Complementary and Alternative Medicine, vol. 2019, p. 1–16, maio 2019, doi: 10.1155/2019/1528635. DOI: https://doi.org/10.1155/2019/1528635
S. Cheikh-Rouhou, S. Besbes, G. Lognay, C. Blecker, C. Deroanne, e H. Attia, “Sterol composition of black cumin (Nigella sativa L.) and Aleppo pine (Pinus halepensis Mill.) seed oils”, Journal of Food Composition and Analysis, vol. 21, no 2, p. 162–168, mar. 2008, doi: 10.1016/j.jfca.2007.09.001. DOI: https://doi.org/10.1016/j.jfca.2007.09.001
B. Nickavar, F. Mojab, K. Javidnia, e M. A. R. Amoli, “Chemical Composition of the Fixed and Volatile Oils of Nigella sativa L. from Iran”, Zeitschrift für Naturforschung C, vol. 58, no 9–10, p. 629–631, out. 2003, doi: 10.1515/znc-2003-9-1004. DOI: https://doi.org/10.1515/znc-2003-9-1004
E. Vassiliou, O. Awoleye, A. Davis, e S. Mishra, “Anti-Inflammatory and Antimicrobial Properties of Thyme Oil and Its Main Constituents”, Int J Mol Sci, vol. 24, no 8, p. 6936, abr. 2023, doi: 10.3390/ijms24086936. DOI: https://doi.org/10.3390/ijms24086936
B. Petrovska, “Historical review of medicinal plants′ usage”, Pharmacogn Rev, vol. 6, no 11, p. 1, 2012, doi: 10.4103/0973-7847.95849. DOI: https://doi.org/10.4103/0973-7847.95849
A. Ahmad et al., “Thymoquinone (2-Isopropyl-5-methyl-1, 4-benzoquinone) as a chemopreventive/anticancer agent: Chemistry and biological effects”, Saudi Pharmaceutical Journal, vol. 27, no 8, p. 1113–1126, dez. 2019, doi: 10.1016/j.jsps.2019.09.008. DOI: https://doi.org/10.1016/j.jsps.2019.09.008
A. B. Dessie, T. D. Koye, A. D. Koye, e A. A. Abitew, “Analysis of red pepper marketing: evidence from northwest Ethiopia”, J Econ Struct, vol. 8, no 1, p. 24, dez. 2019, doi: 10.1186/s40008-019-0156-0. DOI: https://doi.org/10.1186/s40008-019-0156-0
S. H. M. Aljabre, O. M. Alakloby, e M. A. Randhawa, “Dermatological effects of Nigella sativa”, Journal of Dermatology & Dermatologic Surgery, vol. 19, no 2, p. 92–98, jul. 2015, doi: 10.1016/j.jdds.2015.04.002. DOI: https://doi.org/10.1016/j.jdds.2015.04.002
A. Ahmad et al., “A review on therapeutic potential of Nigella sativa: A miracle herb”, Asian Pac J Trop Biomed, vol. 3, no 5, p. 337–352, maio 2013, doi: 10.1016/S2221-1691(13)60075-1. DOI: https://doi.org/10.1016/S2221-1691(13)60075-1
M. Vasam, S. Korutla, e R. A. Bohara, “Acne vulgaris: A review of the pathophysiology, treatment, and recent nanotechnology based advances”, Biochem Biophys Rep, vol. 36, p. 101578, dez. 2023, doi: 10.1016/j.bbrep.2023.101578. DOI: https://doi.org/10.1016/j.bbrep.2023.101578
O. Badary, M. S. Hamza, e R. Tikamdas, “Thymoquinone: A Promising Natural Compound with Potential Benefits for COVID-19 Prevention and Cure”, Drug Des Devel Ther, vol. Volume 15, p. 1819–1833, maio 2021, doi: 10.2147/DDDT.S308863. DOI: https://doi.org/10.2147/DDDT.S308863
D. S. Masson‐Meyers et al., “Experimental models and methods for cutaneous wound healing assessment”, Int J Exp Pathol, vol. 101, no 1–2, p. 21–37, fev. 2020, doi: 10.1111/iep.12346. DOI: https://doi.org/10.1111/iep.12346
S. Wahab e A. Alsayari, “Potential Pharmacological Applications of Nigella Seeds with a Focus on Nigella sativa and Its Constituents against Chronic Inflammatory Diseases: Progress and Future Opportunities”, Plants, vol. 12, no 22, p. 3829, nov. 2023, doi: 10.3390/plants12223829. DOI: https://doi.org/10.3390/plants12223829
A. S. Choudhari, P. C. Mandave, M. Deshpande, P. Ranjekar, e O. Prakash, “Phytochemicals in Cancer Treatment: From Preclinical Studies to Clinical Practice”, Front Pharmacol, vol. 10, jan. 2020, doi: 10.3389/fphar.2019.01614. DOI: https://doi.org/10.3389/fphar.2019.01614
M. Piscione, M. Mazzone, M. C. Di Marcantonio, R. Muraro, e G. Mincione, “Eradication of Helicobacter pylori and Gastric Cancer: A Controversial Relationship”, Front Microbiol, vol. 12, fev. 2021, doi: 10.3389/fmicb.2021.630852. DOI: https://doi.org/10.3389/fmicb.2021.630852
M. A. Al-Azzawi, M. M. N. AboZaid, R. A. L. Ibrahem, e M. A. Sakr, “Therapeutic effects of black seed oil supplementation on chronic obstructive pulmonary disease patients: A randomized controlled double blind clinical trial”, Heliyon, vol. 6, no 8, p. e04711, ago. 2020, doi: 10.1016/j.heliyon.2020.e04711. DOI: https://doi.org/10.1016/j.heliyon.2020.e04711
H. Fallah Huseini et al., “Blood Pressure Lowering Effect of Nigella sativa L. Seed Oil in Healthy Volunteers: A Randomized, Double‐Blind, Placebo‐controlled Clinical Trial”, Phytotherapy Research, vol. 27, no 12, p. 1849–1853, dez. 2013, doi: 10.1002/ptr.4944. DOI: https://doi.org/10.1002/ptr.4944
S. Jarmakiewicz-Czaja, M. Zielińska, K. Helma, A. Sokal, e R. Filip, “Effect of Nigella sativa on Selected Gastrointestinal Diseases”, Curr Issues Mol Biol, vol. 45, no 4, p. 3016–3034, abr. 2023, doi: 10.3390/cimb45040198. DOI: https://doi.org/10.3390/cimb45040198
O. Ketenoglu, S. S. Kiralan, M. Kiralan, G. Ozkan, e M. F. Ramadan, “Cold pressed black cumin (Nigella sativa L.) seed oil”, em Cold Pressed Oils, Elsevier, 2020, p. 53–64. doi: 10.1016/B978-0-12-818188-1.00006-2. DOI: https://doi.org/10.1016/B978-0-12-818188-1.00006-2
K. M. Mousa and S. K. Kouba, “Study on Vanadium Recovery from Spent Catalyst Used in the Manufacture of Sulfuric Acid,” Iraqi Journal of Chemical and Petroleum Engineering, vol. 11, no. 2, pp. 49–54, Jun. 2010, doi: 10.31699/IJCPE.2010.2.6. DOI: https://doi.org/10.31699/IJCPE.2010.2.6
Musa, Khalid Mukhlif, Ali, Isra Shakir Muhammad, Hadi, Hind Jasim. 2012. Extraction of nickel from fly ash of heavy oil using ammonium hydroxide. al-Qadisiyah Journal for Engineering Sciences،Vol.5, no.1, pp.38-43. https://search.emarefa.net/detail/BIM-756958
K. M. Mousa and M. M. Dawood, “Experimental, modelling and kinetic study for the recovery of molybdenum from spent (Ni-Mo/Al2O3) catalyst of hydrotreating process,” in 2012 First National Conference for Engineering Sciences (FNCES 2012), IEEE, Nov. 2012, pp. 1–3. doi: 10.1109/NCES.2012.6740466. DOI: https://doi.org/10.1109/NCES.2012.6740466
Octave Levenspie, Chemical Reaction Engineering, Third Edition, Copyright O 1999 John Wiley & Sons, Inc.
A. C. J. De Korte and H. J. H. Brouwers, “Cellular automata approach to hybrid surface and diffusion controlled reactions,” Reaction Kinetics, Mechanisms and Catalysis, vol. 125, no. 2, pp. 471–492, Dec. 2018, doi: 10.1007/s11144-018-1455-4. DOI: https://doi.org/10.1007/s11144-018-1455-4
Downloads
Published
Issue
Section
License
Copyright (c) 2024 International Journal of Scientific Research in Science, Engineering and Technology
This work is licensed under a Creative Commons Attribution 4.0 International License.
How to Cite
